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SAS experiments carried out at 40 °C to produce PVP-based coprecipitated particles and β-CD-based inclusion complexes (EE = entrapment efficiency, MP = microparticles, NP = nanoparticles, Liq = liquid, and C = crystals).

Journal: Polymers

Article Title: Designing Microparticles of Luteolin and Naringenin in Different Carriers via Supercritical Antisolvent Process

doi: 10.3390/polym16243600

Figure Lengend Snippet: SAS experiments carried out at 40 °C to produce PVP-based coprecipitated particles and β-CD-based inclusion complexes (EE = entrapment efficiency, MP = microparticles, NP = nanoparticles, Liq = liquid, and C = crystals).

Article Snippet: The experiments were conducted using the following materials: carbon dioxide with a purity of 99%, purchased from Morlando Group S.p.A. (Sant’Antimo, Naples, Italy); dimethylsulfoxide (DMSO; purity: 99.5%), delivered by Carlo Erba (Cornaredo, Italy); luteolin (LUT), supplied by Epitech Group (Milan, Italy); and naringenin (NAR), β-cyclodextrin (β-CD; purity: 98%), and polyvinylpyrrolidone (PVP) with a molecular weight of 10 kg/mol, supplied by Sigma Aldrich (Milan, Italy).

Techniques:

Luteolin/β-CD powder precipitated at 150 mg/mL and 1/2 LUT/β-CD molar ratio. The effect of pressure: ( a ) FESEM image at 9 MPa; ( b ) FESEM image at 12 MPa; ( c ) comparison of PSDs.

Journal: Polymers

Article Title: Designing Microparticles of Luteolin and Naringenin in Different Carriers via Supercritical Antisolvent Process

doi: 10.3390/polym16243600

Figure Lengend Snippet: Luteolin/β-CD powder precipitated at 150 mg/mL and 1/2 LUT/β-CD molar ratio. The effect of pressure: ( a ) FESEM image at 9 MPa; ( b ) FESEM image at 12 MPa; ( c ) comparison of PSDs.

Article Snippet: The experiments were conducted using the following materials: carbon dioxide with a purity of 99%, purchased from Morlando Group S.p.A. (Sant’Antimo, Naples, Italy); dimethylsulfoxide (DMSO; purity: 99.5%), delivered by Carlo Erba (Cornaredo, Italy); luteolin (LUT), supplied by Epitech Group (Milan, Italy); and naringenin (NAR), β-cyclodextrin (β-CD; purity: 98%), and polyvinylpyrrolidone (PVP) with a molecular weight of 10 kg/mol, supplied by Sigma Aldrich (Milan, Italy).

Techniques: Comparison

FT-IR spectra of the pure compounds, physical mixtures, and coprecipitated powders: ( a ) LUT/β-CD; ( b ) LUT/PVP; ( c ) NAR/β-CD; ( d ) NAR/PVP.

Journal: Polymers

Article Title: Designing Microparticles of Luteolin and Naringenin in Different Carriers via Supercritical Antisolvent Process

doi: 10.3390/polym16243600

Figure Lengend Snippet: FT-IR spectra of the pure compounds, physical mixtures, and coprecipitated powders: ( a ) LUT/β-CD; ( b ) LUT/PVP; ( c ) NAR/β-CD; ( d ) NAR/PVP.

Article Snippet: The experiments were conducted using the following materials: carbon dioxide with a purity of 99%, purchased from Morlando Group S.p.A. (Sant’Antimo, Naples, Italy); dimethylsulfoxide (DMSO; purity: 99.5%), delivered by Carlo Erba (Cornaredo, Italy); luteolin (LUT), supplied by Epitech Group (Milan, Italy); and naringenin (NAR), β-cyclodextrin (β-CD; purity: 98%), and polyvinylpyrrolidone (PVP) with a molecular weight of 10 kg/mol, supplied by Sigma Aldrich (Milan, Italy).

Techniques: